N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide

Base Information

• Chemical Name: N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide
• CAS No.: 114235-33-5
• Molecular Formula: C₁₇H₁₂Cl₅NO₆S
• Molecular Weight: 535.616

Synonyms:N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide

Chemical Property of N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide

Chemical Property:

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Technology Process of N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide

There total 1 articles about N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)benzenesulfonyl chloride (36898-42-7) + 5,5-dimethoxy-1,2,3,4-tetrachlorocyclopentadiene (2207-27-4) → N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide (114235-33-5)

Guidance literature:

In benzene; for 8h; Heating;

Reference yield: 93.0%

dimethyl amine (124-40-3) + N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide (114235-33-5) → N,N-Dimethyl-4-((2S,6R)-1,7,8,9-tetrachloro-10,10-dimethoxy-3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl)-benzenesulfonamide

Guidance literature:

In methanol; water; for 2h; Ambient temperature;

Reference yield: 92.0%

aniline (62-53-3) + N-(p-chlorosulfonylphenyl)-3,4,5,6-tetrachloro-8,8-dimethoxybicyclo<2.2.1>hept-4-eno succinimide (114235-33-5) → N-Phenyl-4-((1S,2S,6R,7R)-1,7,8,9-tetrachloro-10,10-dimethoxy-3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl)-benzenesulfonamide (114235-35-7)

Guidance literature:

In methanol; water; for 6h; Ambient temperature;

upstream raw materials:

4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)benzenesulfonyl chloride

5,5-dimethoxy-1,2,3,4-tetrachlorocyclopentadiene

Downstream raw materials:

N-Phenyl-4-((1S,2S,6R,7R)-1,7,8,9-tetrachloro-10,10-dimethoxy-3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl)-benzenesulfonamide

C₁₇H₁₅Cl₄N₃O₆S

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