trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene

Base Information

Chemical Name:trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene
CAS No.:137170-74-2
Molecular Formula:C₁₈H₂₂O₂S
Molecular Weight:302.437
Hs Code.:

Synonyms:trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene

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Chemical Property of trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene

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Technology Process of trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene

There total 4 articles about trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 281-23-2
adamantane

: 963-16-6
(E)-1,2-bis(phenylsulfonyl)ethylene

: 137170-74-2
trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene

Guidance literature:: With 1,10-Phenanthroline; copper(l) cyanide; N-(tert-butyl)-N-fluoro-3,5-bis(trifluoromethyl)benzenesulfonamide; In 1,2-dichloro-ethane; at 60 ℃; for 24h; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1021/jacs.1c05874

Reference yield: 40.0%

: 828-51-3
1-Adamantanecarboxylic acid

: 963-16-6
(E)-1,2-bis(phenylsulfonyl)ethylene

: 137170-74-2
trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene

Guidance literature:: With copper acetylacetonate; 1,10-Phenanthroline; N-(tert-butyl)-N-fluoro-3,5-bis(trifluoromethyl)benzamide; In 1,2-dichloro-ethane; at 20 ℃; for 48h; Inert atmosphere; Glovebox; Sealed tube; Irradiation;
DOI:10.1021/jacs.1c05874

Reference yield: 20.0%

: 5535-48-8
PVS

: 80859-83-2
1-benzene

: 126002-57-1
(3r,5r,7r)-1-(2-(phenylsulfonyl)ethyl)adamantane

: 137170-74-2
trans 2-(adamant-1-yl)-1-phenylsulphonyl ethene

: 1,4-di(1-adamantyl)-2,3-di(benzenesulfonyl)butane

Guidance literature:: In dichloromethane; at 30 ℃; for 0.25h; Product distribution; Mechanism; Irradiation; different (diacyloxyiodo)arenes or benzenes, hydrogen donors, olefins, solvent, times and temperatures;
DOI:10.1016/S0040-4020(01)88042-X