tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Base Information

Chemical Name:tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate
CAS No.:1237587-78-8
Molecular Formula:C₂₁H₂₀Cl₂F₃N₃O₃
Molecular Weight:490.309
Hs Code.:

Synonyms:tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

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Chemical Property of tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

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Technology Process of tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

There total 7 articles about tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237587-77-7
tert-butyl {3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbamate

: 1237587-78-8
tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Guidance literature:: With sodium hypochlorite; ammonia; Aliquat 336; ammonium chloride; sodium hydroxide; In tert-butyl methyl ether; water; at 20 ℃; for 12.3333h;

Reference yield:

: 3431-62-7,20747-39-1
3-nitrobenzaldoxime

: 1237587-78-8
tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 - 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 1.25 h / 20 - 75 °C

3.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C

4.1: dmap / tetrahydrofuran / 1.5 h / 20 °C

4.2: 2 h / 20 °C

5.1: sodium hydroxide; sodium hypochlorite; Aliquat 336; ammonia; ammonium chloride / water; tert-butyl methyl ether / 12 h / 20 °C

With sodium hypochlorite; N-chloro-succinimide; ammonia; water; Aliquat 336; iron; ammonium chloride; acetic acid; triethylamine; sodium hydroxide; dmap; In tetrahydrofuran; ethanol; tert-butyl methyl ether; water; N,N-dimethyl-formamide;

Reference yield:

: 1070396-55-2
3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]nitrobenzene

: 1237587-78-8
tert-butyl N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; acetic acid; iron / ethanol / 1.25 h / 20 - 75 °C

2.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C

3.1: dmap / tetrahydrofuran / 1.5 h / 20 °C

3.2: 2 h / 20 °C

4.1: sodium hydroxide; sodium hypochlorite; Aliquat 336; ammonia; ammonium chloride / water; tert-butyl methyl ether / 12 h / 20 °C

With sodium hypochlorite; ammonia; water; Aliquat 336; iron; ammonium chloride; acetic acid; triethylamine; sodium hydroxide; dmap; In tetrahydrofuran; ethanol; tert-butyl methyl ether; water;