N-methyl,N-benzyl furfurylamine

Base Information

• Chemical Name: N-methyl,N-benzyl furfurylamine
• CAS No.: 81404-55-9
• Molecular Formula: C₁₃H₁₅NO
• Molecular Weight: 201.268
• Mol file: 81404-55-9.mol

Synonyms:N-methyl,N-benzyl furfurylamine

Chemical Property of N-methyl,N-benzyl furfurylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-methyl,N-benzyl furfurylamine

There total 12 articles about N-methyl,N-benzyl furfurylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

→ N-methyl,N-benzyl furfurylamine (81404-55-9)

Guidance literature:

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; at 20 ℃;

Reference yield: 75.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N-benzyl(furan-2-ylmethyl)amine (4439-53-6) → N-methyl,N-benzyl furfurylamine (81404-55-9)

Guidance literature:

With sodium cyanoborohydride; acetic acid; In water; acetonitrile; at 20 ℃;

DOI:10.1016/j.poly.2014.03.041

Reference yield: 68.0%

N-methyl-2-furanmethanamine (4753-75-7) + benzyl alcohol (100-51-6,185532-71-2) → N-methyl,N-benzyl furfurylamine (81404-55-9)

Guidance literature:

With polystyrene supported triphenylphosphine ruthenium complex; In toluene; at 140 ℃; for 24h; Sealed tube; Flow reactor;

DOI:10.1002/cctc.201300971

upstream raw materials:

N,N'-dimethylbenzylamine

(furan-2-ylmethyl)dimethylamine

methyl iodide

formaldehyd

Downstream raw materials:

2-bromomethylfuran

Refernces

• 1、 -. "Multimodal Anion Exchange Matrices". Paragraph 0081; 0083; 0084; 0089. . Retrieved 2015/11/23.
• 2、 Peishan, Siah,Dang, Tuan Thanh,Seayad, Abdul Majeed,Ramalingam, Balamurugan. "Reusable supported ruthenium catalysts for the alkylation of amines by using primary alcohols". . p. 808 - 814. Retrieved 2014/03/21.