16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane

Base Information

Chemical Name:16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane
CAS No.:753454-06-7
Molecular Formula:C₃₇H₄₁NO₆
Molecular Weight:595.736
Hs Code.:

Synonyms:16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane

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Chemical Property of 16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane

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Technology Process of 16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane

There total 3 articles about 16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 135-19-3
β-naphthol

: 753454-05-6
1-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadec-16-yl)phenyl]-1-phenylprop-2-yn-1-ol

: 753454-06-7
16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 60 - 80 ℃; for 3h;
DOI:10.1023/B:RUCB.0000019883.50477.cc

Reference yield:

: 93-98-1,5705-51-1
N-phenyl benzoyl amide

: 753454-06-7
16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 12 percent / POCl₃ / 4 h / 100 °C

2: 90 percent / tetrahydrofuran / 3 h / 60 °C

3: 35 percent / TsOH*H₂O / toluene / 3 h / 60 - 80 °C

With toluene-4-sulfonic acid; trichlorophosphate; In tetrahydrofuran; toluene;
DOI:10.1023/B:RUCB.0000019883.50477.cc

Reference yield:

: 245125-21-7
[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadec-16-yl)phenyl]phenylmethanone

: 753454-06-7
16-[4-(2-phenyl-2H-benzo[f]chromen-2-yl)phenyl]-1,4,7,10,13-pentaoxa-16-azacyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran / 3 h / 60 °C

2: 35 percent / TsOH*H₂O / toluene / 3 h / 60 - 80 °C

With toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1023/B:RUCB.0000019883.50477.cc