3-nitrosoveratrole

Base Information

Chemical Name:3-nitrosoveratrole
CAS No.:121001-03-4
Molecular Formula:C₈H₉NO₃
Molecular Weight:167.164
Hs Code.:

Synonyms:3-nitrosoveratrole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-nitrosoveratrole

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Technology Process of 3-nitrosoveratrole

There total 3 articles about 3-nitrosoveratrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 6299-67-8
2,3-dimethoxyaniline

: 121001-03-4
3-nitrosoveratrole

Guidance literature:: With manganese(II) sulfate; sodium tungstate; dihydrogen peroxide; In water;

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 121001-03-4
3-nitrosoveratrole

Guidance literature:: Multi-step reaction with 3 steps

1: 2.5 M n-butyllithium / diethyl ether; hexane / 48 h / Ambient temperature

2: 1.) p-toluenesulfonyl azide; 2.) tetrabutylammonium hydrogen sulfate, sodium borohydride / 1.) ether, -78 deg C, 5 h; 2.) water, rt to 30 deg C

3: 72 percent / Na₂WO₄*2H₂O/MnSO₄*7H₂O, 30percent H₂O₂ / H₂O

With sodium tetrahydroborate; manganese(II) sulfate; sodium tungstate; n-butyllithium; 4-toluenesulfonyl azide; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate; In diethyl ether; hexane; water;

Reference yield:

: 2785-95-7
3-lithio-1,2-dimethoxybenzene

: 121001-03-4
3-nitrosoveratrole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) p-toluenesulfonyl azide; 2.) tetrabutylammonium hydrogen sulfate, sodium borohydride / 1.) ether, -78 deg C, 5 h; 2.) water, rt to 30 deg C

2: 72 percent / Na₂WO₄*2H₂O/MnSO₄*7H₂O, 30percent H₂O₂ / H₂O

With sodium tetrahydroborate; manganese(II) sulfate; sodium tungstate; 4-toluenesulfonyl azide; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate; In water;