2,2'-diphenyl-5,5'-bisbenzimidazolyl ether

Base Information

Chemical Name:2,2'-diphenyl-5,5'-bisbenzimidazolyl ether
CAS No.:73672-91-0
Molecular Formula:C₂₆H₁₈N₄O
Molecular Weight:402.455
Hs Code.:

Synonyms:2,2'-diphenyl-5,5'-bisbenzimidazolyl ether

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Chemical Property of 2,2'-diphenyl-5,5'-bisbenzimidazolyl ether

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Technology Process of 2,2'-diphenyl-5,5'-bisbenzimidazolyl ether

There total 6 articles about 2,2'-diphenyl-5,5'-bisbenzimidazolyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.9%

: 434-45-7
2,2,2-Trifluoroacetophenone

: 2676-59-7
bis(3,4-diaminophenyl)ether

: 73672-91-0
2,2'-diphenyl-5,5'-bisbenzimidazolyl ether

Guidance literature:: In N,N-dimethyl acetamide; at 120 - 130 ℃; for 24h;
DOI:10.1081/SCC-120015562

Reference yield: 64.6%

: 100-52-7
benzaldehyde

: 2676-59-7
bis(3,4-diaminophenyl)ether

: 73672-91-0
2,2'-diphenyl-5,5'-bisbenzimidazolyl ether

Guidance literature:: With sodium hydrogensulfite; In methanol; for 8h;
DOI:10.1016/j.bmcl.2012.06.102

Reference yield:

: 3070-86-8
N-[4-(4-acetylaminophenoxy)phenyl]acetamide

: 73672-91-0
2,2'-diphenyl-5,5'-bisbenzimidazolyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid; acetic acid

2: potassium hydroxide; water / methanol / Reflux

3: 10% Pd/C; hydrogen / methanol / 20 °C

4: sodium hydrogensulfite / methanol / 8 h

With 10% Pd/C; water; hydrogen; nitric acid; sodium hydrogensulfite; acetic acid; potassium hydroxide; In methanol;
DOI:10.1016/j.bmcl.2012.06.102