N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine

Base Information

Chemical Name:N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine
CAS No.:1377585-42-6
Molecular Formula:C₂₀H₂₇NO₃SSi
Molecular Weight:389.591
Hs Code.:

Synonyms:N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine

Chemical Property:

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Technology Process of N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine

There total 2 articles about N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 160907-95-9
3-((tert-butyldimethylsilyl)oxy)benzoic acid

: 4381-25-3
S-methyl-S-phenylsulfoximine

: 1377585-42-6
N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201200092

Reference yield:

: 1193-82-4
racemic methyl phenyl sulfoxide

: 1377585-42-6
N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide; sulfuric acid / chloroform / Inert atmosphere

1.2: 12 h / 0 - 45 °C

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium azide; sulfuric acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; chloroform;
DOI:10.1002/chem.201200092

Reference yield: 47.0%

: 1377585-42-6
N-[3-(tert-butyldimethylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine

: 64-19-7,77671-22-8
acetic acid

: 1377585-10-8
N-[2-acetoxy-5-(tert-butyldiphenylsilyloxy)benzoyl]-S-methyl-S-phenylsulfoximine

Guidance literature:: With dipotassium peroxodisulfate; palladium diacetate; In chloroform; at 100 ℃; for 48h; air;
DOI:10.1002/chem.201200092