methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate

Base Information

• Chemical Name: methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate
• CAS No.: 1381766-62-6
• Molecular Formula: C₂₅H₃₆N₆O₅
• Molecular Weight: 500.598

Synonyms:methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate

Chemical Property of methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate

Chemical Property:

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Technology Process of methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate

There total 1 articles about methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetic acid (1381766-60-4) → methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate (1381766-62-6)

Guidance literature:

With chloro-trimethyl-silane; at 20 ℃; for 1h;

Reference yield:

methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate (1381766-62-6) → [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetic acid (1381766-60-4)

Guidance literature:

With sodium tris(acetoxy)borohydride; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 16.1667h;

Reference yield:

methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetate (1381766-62-6) + methanesulfonyl chloride (124-63-0) → methyl {4-[([3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]{3-[(methylsulfonyl)oxy]propyl}amino)methyl]phenyl}acetate (1381766-64-8)

Guidance literature:

With triethylamine; In dichloromethane; for 5h;

upstream raw materials:

methanol

[4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-hydroxypropyl)amino}methyl)phenyl]acetic acid

Downstream raw materials:

methyl {4-[([3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl]{3-[(methylsulfonyl)oxy]propyl}amino)methyl]phenyl}acetate

methyl [4-{[[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-piperidin-1-ylpropyl)amino]methyl}phenyl]acetate hydrobromide

methyl [3-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl](3-chloropropyl)amino}methyl)phenyl]acetate

methyl [4-({[3-(6-amino-2-butoxy-8-oxo-7,8-dihydro-9H-purin-9-yl)propyl][3-(piperidin-1-yl)propyl]amino}methyl)phenyl]acetate

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