methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate

Base Information

Chemical Name:methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate
CAS No.:1544664-00-7
Molecular Formula:C₂₀H₁₈F₆O₃
Molecular Weight:420.352
Hs Code.:

Synonyms:methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate

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Technology Process of methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate

There total 7 articles about methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1544663-98-0
6-bromo-1-(trifluoromethyl)-2-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalene

: 1544664-00-7
methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine; at 100 ℃; for 4h; under 11400.8 Torr; Autoclave;

Reference yield:

: 1544663-95-7
6-bromo-1-iodo-2-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalene

: 1544664-00-7
methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 85 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine / 4 h / 100 °C / 11400.8 Torr / Autoclave

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; triethylamine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

: 1544665-15-7
2-bromo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalene

: 1544664-00-7
methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; trifluoroacetic acid / acetonitrile / 20 °C

2: copper(l) iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 85 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine / 4 h / 100 °C / 11400.8 Torr / Autoclave

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-iodo-succinimide; copper(l) iodide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In N,N-dimethyl-formamide; acetonitrile;