2-bromoethyl p-phenyl ether

Base Information

• Chemical Name: 2-bromoethyl p-phenyl ether
• CAS No.: 190366-51-9
• Molecular Formula: C₃₉H₄₇BrO
• Molecular Weight: 611.706
• Mol file: 190366-51-9.mol

Synonyms:2-bromoethyl p-phenyl ether

Chemical Property of 2-bromoethyl p-phenyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-bromoethyl p-phenyl ether

There total 8 articles about 2-bromoethyl p-phenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-methanesulfonylethyl p-phenyl ether (224784-43-4) → 2-bromoethyl p-phenyl ether (190366-51-9)

Guidance literature:

With lithium bromide; In acetone; for 2h; Heating;

DOI:10.1021/ja984051w

Reference yield: 46.0%

4-[tris-(4-tert-butylphenyl)methyl]phenol (143998-20-3) + ethylene dibromide (106-93-4) → 2-bromoethyl p-phenyl ether (190366-51-9)

Guidance literature:

With potassium carbonate; In acetone; at 45 ℃;

DOI:10.1002/anie.202104924

Reference yield:

2-hydroxyethyl p-phenyl ether (224784-42-3) → 2-bromoethyl p-phenyl ether (190366-51-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / Et₃N / CH₂Cl₂ / 3.5 h / -2 °C

2: 100 percent / LiBr / acetone / 2 h / Heating

With triethylamine; lithium bromide; In dichloromethane; acetone;

DOI:10.1021/ja984051w

upstream raw materials:

2-methanesulfonylethyl p-phenyl ether

4-[tris-(4-tert-butylphenyl)methyl]phenol

2-hydroxyethyl p-phenyl ether

tris(4-(tert-butyl)phenyl)methanol

Downstream raw materials:

(C₅H₄FeC₅H₄(CONHCH₂C₅H₄N)2)2Cu⁽¹⁺⁾

(C₅H₅FeC₅H₄CHC(C₅H₄N)2)2Cu⁽¹⁺⁾

1-(2-azidoethoxy)-4-(tris(4-tert-butylphenyl)methyl)benzene

Refernces

• 1、 Armaroli, Nicola,Balzani, Vincenzo,Collin, Jean-Paul,Gavina, Pablo,Sauvage, Jean-Pierre,Ventura, Barbara. "Rotaxanes incorporating two different coordinating units in their thread: Synthesis and electrochemically and photochemically induced molecular motions". . p. 4397 - 4408. Retrieved 2007/10/03.