methyl 2-amino-3-methoxy-6-methylbenzoate

Base Information

Chemical Name:methyl 2-amino-3-methoxy-6-methylbenzoate
CAS No.:157485-02-4
Molecular Formula:C₁₅H₁₉NO₆
Molecular Weight:309.319
Hs Code.:

methyl 2-<N-formyl-N-(1-methoxycarbonylethyl)>amino-3-methoxy-6-methylbenzoate

Synonyms:methyl 2-amino-3-methoxy-6-methylbenzoate

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Chemical Property of methyl 2-amino-3-methoxy-6-methylbenzoate

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Technology Process of methyl 2-amino-3-methoxy-6-methylbenzoate

There total 6 articles about methyl 2-amino-3-methoxy-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 64-18-6
formic acid

: 157485-01-3
methyl 3-methoxy-2-(1-methoxycarbonylethyl)amino-6-methylbenzoate

: 157485-02-4
methyl 2-amino-3-methoxy-6-methylbenzoate

Guidance literature:: With acetic anhydride; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(01)86993-3

Reference yield:

: 120-71-8
Cresidine

: 157485-02-4
methyl 2-amino-3-methoxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / Et₂NPh / benzene / 24 h / Heating

2: 2.) TiCl₄ / 1.) CH₂Cl₂, 2 h, room temp., 2.) CH₂Cl₂, -10 deg C; overnight, 12 deg C

3: 40percent KOH, 35percent H₂O₂ / 2 h / Ambient temperature

4: SOCl₂ / 5 h / 0 °C

5: K₂CO₃ / dimethylformamide / 1 h / 0 °C

6: 98 percent / Ac₂O / CH₂Cl₂ / Ambient temperature

With potassium hydroxide; thionyl chloride; dihydrogen peroxide; acetic anhydride; titanium tetrachloride; potassium carbonate; N,N-diethylaniline; In dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4020(01)86993-3

Reference yield:

: 157484-98-5
1-methoxy-2-(1-methoxycarbonylethyl)amino-4-methylbenzene

: 157485-02-4
methyl 2-amino-3-methoxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 2.) TiCl₄ / 1.) CH₂Cl₂, 2 h, room temp., 2.) CH₂Cl₂, -10 deg C; overnight, 12 deg C

2: 40percent KOH, 35percent H₂O₂ / 2 h / Ambient temperature

3: SOCl₂ / 5 h / 0 °C

4: K₂CO₃ / dimethylformamide / 1 h / 0 °C

5: 98 percent / Ac₂O / CH₂Cl₂ / Ambient temperature

With potassium hydroxide; thionyl chloride; dihydrogen peroxide; acetic anhydride; titanium tetrachloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)86993-3