2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine

Base Information

• Chemical Name: 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine
• CAS No.: 1313884-70-6
• Molecular Formula: C₁₉H₂₆ClN
• Molecular Weight: 303.875

Synonyms:2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine

Chemical Property of 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine

There total 3 articles about 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)ethanamine (1313885-05-0) → 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine (1313884-70-6)

Guidance literature:

formaldehyd; 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)ethanamine; With formic acid; In water; Reflux;

With sodium hydroxide; In water;

DOI:10.1016/j.bmc.2011.04.035

Reference yield:

myrtenal (564-94-3,18486-69-6) → 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine (1313884-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 48 h / 20 °C

1.2: 0.17 h

2.1: formic acid / water / Reflux

With formic acid; sodium tris(acetoxy)borohydride; In water; 1,2-dichloro-ethane; 2.1: Eschweiler-Clarke reaction;

DOI:10.1016/j.bmc.2011.04.035

Reference yield:

4-chlorophenylethylamine (156-41-2) → 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine (1313884-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 48 h / 20 °C

1.2: 0.17 h

2.1: formic acid / water / Reflux

With formic acid; sodium tris(acetoxy)borohydride; In water; 1,2-dichloro-ethane; 2.1: Eschweiler-Clarke reaction;

DOI:10.1016/j.bmc.2011.04.035

upstream raw materials:

formaldehyd

2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)ethanamine

myrtenal

4-chlorophenylethylamine

Downstream raw materials:

2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide

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