2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide

Base Information

Chemical Name:2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide
CAS No.:1313884-31-9
Molecular Formula:C₂₀H₂₉ClN*I
Molecular Weight:445.814
Hs Code.:

Synonyms:2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide

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Chemical Property of 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide

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Technology Process of 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide

There total 4 articles about 2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1313884-70-6
2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N-methylethanamine

: 74-88-4
methyl iodide

: 1313884-31-9
2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide

Guidance literature:: In dichloromethane; at 20 ℃; Inert atmosphere; Darkness;
DOI:10.1016/j.bmc.2011.04.035

Reference yield:

: 1313885-05-0
2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)ethanamine

: 1313884-31-9
2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid / water / Reflux

2: dichloromethane / 20 °C / Inert atmosphere; Darkness

With formic acid; In dichloromethane; water; 1: Eschweiler-Clarke reaction;
DOI:10.1016/j.bmc.2011.04.035

Reference yield:

: 564-94-3,18486-69-6
myrtenal

: 1313884-31-9
2-(4-chlorophenyl)-N-(((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methyl)-N,N-dimethylethanaminium iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 48 h / 20 °C

1.2: 0.17 h

2.1: formic acid / water / Reflux

3.1: dichloromethane / 20 °C / Inert atmosphere; Darkness

With formic acid; sodium tris(acetoxy)borohydride; In dichloromethane; water; 1,2-dichloro-ethane; 2.1: Eschweiler-Clarke reaction;
DOI:10.1016/j.bmc.2011.04.035