2-(4-chlorophenyloxy)-2-(4-chlorophenyl)-5-methyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane

Base Information

Chemical Name:2-(4-chlorophenyloxy)-2-(4-chlorophenyl)-5-methyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane
CAS No.:95890-68-9
Molecular Formula:C₁₉H₂₂BCl₂NO₂
Molecular Weight:378.106
Hs Code.:

Synonyms:2-(4-chlorophenyloxy)-2-(4-chlorophenyl)-5-methyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane

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Chemical Property of 2-(4-chlorophenyloxy)-2-(4-chlorophenyl)-5-methyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane

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Technology Process of 2-(4-chlorophenyloxy)-2-(4-chlorophenyl)-5-methyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane

There total 1 articles about 2-(4-chlorophenyloxy)-2-(4-chlorophenyl)-5-methyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 95890-53-2
2,2-bis(4-chlorophenyl)-6-methyl-4,4-tetramethylene-1,3-dioxa-4-azonia-2-boratacyclohexane

: 95890-68-9
2-(4-chlorophenyloxy)-2-(4-chlorophenyl)-5-methyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane

Guidance literature:: In xylene; borate was suspended in anhyd. xylene followed by heating until clear soln. formed; cooled, xylene was evapd., residue treated with anhyd. ether, recrystd. from ether; elem. anal.;
DOI:10.1016/0022-328X(84)80698-1

Reference yield:

: 95890-68-9
2-(4-chlorophenyloxy)-2-(4-chlorophenyl)-5-methyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane

: 95-57-8
2-monochlorophenol

: 1679-18-1
4-Chlorophenylboronic acid

Guidance literature:: With water; In methanol; water; byproducts: 4-chlorophenol, 1-pyrrilidino-2-propanol; borate was suspended in boiling water, dild. with methanol until dissolution of the ppt.; cooled, mixt. was analyzed by TLC (SiO2, dioxane-benzene-AcOH);
DOI:10.1016/0022-328X(84)80698-1