N-benzylidene-α-valine ethylester

Base Information

Chemical Name:N-benzylidene-α-valine ethylester
CAS No.:60930-32-7
Molecular Formula:C₁₄H₁₉NO₂
Molecular Weight:233.31
Hs Code.:

Synonyms:N-benzylidene-α-valine ethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzylidene-α-valine ethylester

Chemical Property:

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Technology Process of N-benzylidene-α-valine ethylester

There total 2 articles about N-benzylidene-α-valine ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 40682-54-0
ethyl N-benzylideneglycinate

: 75-26-3
isopropyl bromide

: 60930-32-7
N-benzylidene-α-valine ethylester

Guidance literature:: With potassium hydroxide; potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride; In acetonitrile; for 8h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86041-5

Reference yield:

: 75-30-9
2-iodo-propane

: 40682-54-0
ethyl N-benzylideneglycinate

: 60930-32-7
N-benzylidene-α-valine ethylester

Guidance literature:: Multistep reaction; (i) LDA, THF, HMPA, (ii) /BRN= 1098244/;
DOI:10.1021/jo00883a044

Reference yield:

: 60930-32-7
N-benzylidene-α-valine ethylester

: 516-06-3,25609-85-2,7004-03-7,921-10-8
D,L-valine

Guidance literature:: With hydrogenchloride; Yield given. Multistep reaction; 1.) ether, 12 h, room temp.; 2.) reflux, 4 h;
DOI:10.1016/S0040-4020(01)86041-5