N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester

Base Information

Chemical Name:N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester
CAS No.:862158-41-6
Molecular Formula:C₁₃H₁₇N₅O₂
Molecular Weight:275.31
Hs Code.:

Synonyms:N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester

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Chemical Property of N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester

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Technology Process of N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester

There total 2 articles about N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 179421-16-0
4-(4-iodo-phenyl)-4H-[1,2,4]triazole

: 862158-41-6
N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 68h;
DOI:10.1021/jo050464l

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 862158-41-6
N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / TMS-Cl; pyridine / 12 h / Heating

2: 48 percent / CuI; 1,10-phenanthroline; Cs₂CO₃ / dimethylformamide / 68 h / 80 °C

With pyridine; copper(l) iodide; chloro-trimethyl-silane; 1,10-Phenanthroline; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jo050464l

Reference yield: 51.0%

: 862158-41-6
N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester

: 862158-39-2
1-but-3-enyl-4-[2-(3-fluoro-phenyl)-ethyl]piperazine

: 201230-82-2
carbon monoxide

: 188400-51-3
L-775606

Guidance literature:: N-(4-[1,2,4]-triazol-4-yl-phenyl)-hydrazinecarboxylic acud tert-butyl ester; 1-but-3-enyl-4-[2-(3-fluoro-phenyl)-ethyl]piperazine; carbon monoxide; With hydrogen; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; Rh(acac)2(CO)2; In tetrahydrofuran; at 70 ℃; for 72h; under 15001.2 Torr;

With sulfuric acid; for 2h; Heating;
DOI:10.1021/jo050464l