1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene

Base Information

Chemical Name:1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene
CAS No.:83637-52-9
Molecular Formula:C₂₃H₂₆O₃S
Molecular Weight:382.524
Hs Code.:

Synonyms:1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene

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Chemical Property of 1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene

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Technology Process of 1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene

There total 5 articles about 1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1121-18-2
2-methyl-2-cyclohexen-1-one

: 83637-51-8
5-methoxybenzocyclobut-1-enylmethyl phenyl sulphoxide

: 83637-52-9
1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 1h;

Reference yield:

: 30267-36-8
5-methoxybenzocyclobuten-1-yl toluene-p-sulphonate

: 83637-52-9
1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide

2: m-chloroperbenzoic acid / CH₂Cl₂

3: 38 percent / lithium di-isopropylamide / tetrahydrofuran

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39820000699

Reference yield:

: 83637-50-7
5-methoxybenzocyclobut-1-enyl phenyl sulphide

: 83637-52-9
1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 2 steps

1: m-chloroperbenzoic acid / CH₂Cl₂

2: 38 percent / lithium di-isopropylamide / tetrahydrofuran

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c39820000699