S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

Base Information

Chemical Name:S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate
CAS No.:1345983-66-5
Molecular Formula:C₁₉H₂₀BrNO₃S
Molecular Weight:422.343
Hs Code.:

Synonyms:S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

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Chemical Property of S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

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Technology Process of S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

There total 5 articles about S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1345983-69-8
O-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

: 1345983-66-5
S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

Guidance literature:: In diphenylether; at 215 ℃; for 4.5h;

Reference yield:

: 98-88-4
benzoyl chloride

: 1345983-66-5
S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 49 h / 5 - 20 °C / Reflux

2.1: boron trichloride / dichloromethane / 0.5 h / 0 - 5 °C

2.2: 0.5 h / 10 °C

2.3: 0.5 h / 15 °C

3.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.75 h / 0 - 20 °C

3.2: 3 h / 60 °C

4.1: diphenylether / 4.5 h / 215 °C

With trifluorormethanesulfonic acid; potassium tert-butylate; boron trichloride; In diphenylether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 25245-34-5
1-bromo-2,5-dimethoxybenzene

: 1345983-66-5
S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 49 h / 5 - 20 °C / Reflux

2.1: boron trichloride / dichloromethane / 0.5 h / 0 - 5 °C

2.2: 0.5 h / 10 °C

2.3: 0.5 h / 15 °C

3.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.75 h / 0 - 20 °C

3.2: 3 h / 60 °C

4.1: diphenylether / 4.5 h / 215 °C

With trifluorormethanesulfonic acid; potassium tert-butylate; boron trichloride; In diphenylether; dichloromethane; N,N-dimethyl-formamide;