[2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone

Base Information

Chemical Name:[2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone
CAS No.:1345983-70-1
Molecular Formula:C₂₄H₃₂BrNO₂S
Molecular Weight:478.494
Hs Code.:

Synonyms:[2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone

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Chemical Property of [2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone

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Technology Process of [2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone

There total 11 articles about [2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 393855-85-1
2-amino-2-butylhexanyl hydrogen sulfate

: 1345983-66-5
S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

: 1345983-70-1
[2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone

Guidance literature:: S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate; With potassium hydroxide; In ethanol; water; at 70 ℃; for 18h; Reflux;

2-amino-2-butylhexanyl hydrogen sulfate; In ethanol; water; at 85 ℃; for 15h;

Reference yield:

: 393855-78-2
2-amino-2-butyl-hexanoic acid ethyl ester

: 1345983-70-1
[2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 65 °C

1.2: 2 h / 0 °C

2.1: chlorosulfonic acid / ethyl acetate / 3 h / 25 - 40 °C

3.1: potassium hydroxide / ethanol; water / 18 h / 70 °C / Reflux

3.2: 15 h / 85 °C

With chlorosulfonic acid; lithium aluminium tetrahydride; potassium hydroxide; In tetrahydrofuran; ethanol; water; ethyl acetate;

Reference yield:

: 98-88-4
benzoyl chloride

: 1345983-70-1
[2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 49 h / 5 - 20 °C / Reflux

2.1: boron trichloride / dichloromethane / 0.5 h / 0 - 5 °C

2.2: 0.5 h / 10 °C

2.3: 0.5 h / 15 °C

3.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.75 h / 0 - 20 °C

3.2: 3 h / 60 °C

4.1: diphenylether / 4.5 h / 215 °C

5.1: potassium hydroxide / ethanol; water / 18 h / 70 °C / Reflux

5.2: 15 h / 85 °C

With trifluorormethanesulfonic acid; potassium tert-butylate; boron trichloride; potassium hydroxide; In diphenylether; ethanol; dichloromethane; water; N,N-dimethyl-formamide;