ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate

Base Information

Chemical Name:ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate
CAS No.:1072709-39-7
Molecular Formula:C₂₁H₃₀O₅
Molecular Weight:362.466
Hs Code.:

Synonyms:ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate

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Chemical Property of ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate

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Technology Process of ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate

There total 7 articles about ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 1072709-37-5
4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexanone

: 1072709-39-7
ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate

Guidance literature:: 4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexanone; With sodium hydride; In tetrahydrofuran; at 18 ℃; for 0.0833333h;

diethoxyphosphoryl-acetic acid ethyl ester; In tetrahydrofuran; for 2.5h;

Reference yield:

: 22428-87-1
4,4-ethylenedioxycyclohexan-1-ol

: 1072709-39-7
ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 5 h / 0 °C

2.1: N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C

2.2: 0.5 h / -78 °C

2.3: -78 - 18 °C

3.1: hydrogenchloride; water / tetrahydrofuran / 24 h / 18 °C

4.1: sodium hydride / tetrahydrofuran / 0.08 h / 18 °C

4.2: 2.5 h

With hydrogenchloride; carbon tetrabromide; N,N,N,N,-tetramethylethylenediamine; water; tert.-butyl lithium; sodium hydride; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; pentane;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1072709-39-7
ethyl 2-{4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexylidene}acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate / methanol / 1 h / 0 - 18 °C

2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 5 h / 0 °C

3.1: N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C

3.2: 0.5 h / -78 °C

3.3: -78 - 18 °C

4.1: hydrogenchloride; water / tetrahydrofuran / 24 h / 18 °C

5.1: sodium hydride / tetrahydrofuran / 0.08 h / 18 °C

5.2: 2.5 h

With hydrogenchloride; sodium tetrahydroborate; carbon tetrabromide; N,N,N,N,-tetramethylethylenediamine; water; tert.-butyl lithium; sodium hydride; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; pentane;