N,N'-Diacetylbenzidine

Base Information

Chemical Name:N,N'-Diacetylbenzidine
CAS No.:613-35-4
Molecular Formula:C16H16 N2 O2
Molecular Weight:268.315
Hs Code.:2924299090
European Community (EC) Number:210-338-2
ICSC Number:1678
NSC Number:12409,4717
UNII:2EE5599GQS
DSSTox Substance ID:DTXSID9036854
Nikkaji Number:J36.102J
Wikidata:Q26840865
ChEMBL ID:CHEMBL1567221
Mol file:613-35-4.mol

Synonyms:N,N'-diacetylbenzidine

Suppliers and Price of N,N'-Diacetylbenzidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Diacetylbenzidine
10g
$ 425.00

TRC
Diacetylbenzidine
1g
$ 110.00

Sigma-Aldrich
N-(4'-ACETYLAMINO-BIPHENYL-4-YL)-ACETAMIDE AldrichCPR
1ea
$ 57.00

Medical Isotopes, Inc.
Diacetylbenzidine
125 g
$ 1800.00

Biosynth Carbosynth
Diacetylbenzidine
25 g
$ 700.00

Biosynth Carbosynth
Diacetylbenzidine
10 g
$ 440.00

Biosynth Carbosynth
Diacetylbenzidine
5 g
$ 300.00

Biosynth Carbosynth
Diacetylbenzidine
2 g
$ 200.00

Biosynth Carbosynth
Diacetylbenzidine
1 g
$ 150.00

Aronis compounds
N,N'-4,4'-biphenyldiyldiacetamide
100mg
$ 80.00

Total 15 raw suppliers

Chemical Property of N,N'-Diacetylbenzidine

Chemical Property:

Melting Point:317°C
Refractive Index:1.6240 (estimate)
Boiling Point:411.48°C (rough estimate)
PKA:14.60±0.70(Predicted)
Flash Point:251.9oC
PSA：58.20000
Density:1.1028 (rough estimate)
LogP:3.41640
Storage Temp.:Amber Vial, -20°C Freezer, Under inert atmosphere
Solubility.:DMSO (Slightly)
XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:268.121177757
Heavy Atom Count:20
Complexity:306

Purity/Quality:

99.5% ^*data from raw suppliers

Diacetylbenzidine ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 20/21/22
Safety Statements: 22-36

MSDS Files:: SDS file from LookChem

Useful:

Chemical Classes:Nitrogen Compounds -> Benzidine and Derivatives
Canonical SMILES:CC(=O)NC1=CC=C(C=C1)C2=CC=C(C=C2)NC(=O)C
Inhalation Risk:A harmful concentration of airborne particles can be reached quickly when dispersed.
Effects of Short Term Exposure:May cause mechanical irritation to the eyes and respiratory tract.
Effects of Long Term Exposure:The substance may have effects on the blood and kidneys. This may result in the formation of methaemoglobin, anaemia and kidney impairment. This substance is possibly carcinogenic to humans.
Uses Diacetylbenzidine (cas# 613-35-4) is a compound useful in organic synthesis.

Technology Process of N,N'-Diacetylbenzidine

There total 15 articles about N,N'-Diacetylbenzidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 92-87-5
p,p'-diaminobiphenyl

: 613-35-4
N,N'-Diacetylbenzidin

Guidance literature:: DOI:10.1016/0165-1218(93)90027-B

Reference yield: 85.0%

: 622-50-4
4-Acetamido-1-iodobenzene

: 613-35-4
N,N'-Diacetylbenzidin

Guidance literature:: With dipotassium hydrogenphosphate; digold(I)bis(diphenylphosphinomethane)dichloride; triethylamine; In methanol; acetonitrile; for 16h; Inert atmosphere; UV-irradiation;
DOI:10.1021/acs.orglett.6b02021

Reference yield: 50.0%

: 121-60-8
p-acetylaminobenzenesulfonyl chloride

: 613-35-4
N,N'-Diacetylbenzidin

Guidance literature:: With copper(l) iodide; palladium diacetate; sodium hydrogencarbonate; triphenylphosphine; silver carbonate; In 1,4-dioxane; for 4h; Reflux; Schlenk technique;
DOI:10.1002/cjoc.201400868