<(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

Base Information

Chemical Name:<(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)
CAS No.:102192-13-2
Molecular Formula:C₁₉H₂₅N₃O₉
Molecular Weight:439.422
Hs Code.:

Synonyms:<(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

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Chemical Property of <(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

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Technology Process of <(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

There total 4 articles about <(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7352-64-9
glycine 4-nitrobenzyl ester

: 102192-13-2
<(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) magnesium sulfate 2.) triethylamine / 1.) CH₂Cl₂, 30 min, room temp. 2.) CH₂Cl₂, 30 min, reflux

2: 97 percent / hydrazine hydrate / dioxane / 1 h / Ambient temperature

3: 63 percent / tetrahydrofuran / 1 h / Heating

4: 1.) ozone 2.) dimethyl sulfide / 1.) CH₂Cl₂, -70 deg C 2.) CH₂Cl₂, 1 h, room temp.

With dimethylsulfide; magnesium sulfate; ozone; hydrazine hydrate; triethylamine; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 102192-12-1
[(3S,4R)-3-Amino-2-oxo-4-((E)-styryl)-azetidin-1-yl]-acetic acid 4-nitro-benzyl ester

: 102192-13-2
<(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / tetrahydrofuran / 1 h / Heating

2: 1.) ozone 2.) dimethyl sulfide / 1.) CH₂Cl₂, -70 deg C 2.) CH₂Cl₂, 1 h, room temp.

With dimethylsulfide; ozone; In tetrahydrofuran;

Reference yield:

: 102192-11-0
oxo-2 (phenyl-2 vinyl)-4 phtalimido-3 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-S,R)(E)

: 102192-13-2
<(tert-butoxycarbonyl)amino>-3 (hydroxymethoxymethyl)-4 oxo-2 azetidine-1-acetate de p-nitrobenzyle (3-R,S)(4-R,S)

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / hydrazine hydrate / dioxane / 1 h / Ambient temperature

2: 63 percent / tetrahydrofuran / 1 h / Heating

3: 1.) ozone 2.) dimethyl sulfide / 1.) CH₂Cl₂, -70 deg C 2.) CH₂Cl₂, 1 h, room temp.

With dimethylsulfide; ozone; hydrazine hydrate; In tetrahydrofuran; 1,4-dioxane;