sodium{(THF)4.9} hexacarbonyltantalate

Base Information

Chemical Name:sodium{(THF)4.9} hexacarbonyltantalate
CAS No.:15602-40-1
Molecular Formula:C₄H₈O*C₆O₆Ta*Na
Molecular Weight:725.324
Hs Code.:

Synonyms:sodium{(THF)4.9} hexacarbonyltantalate

Suppliers and Price of sodium{(THF)4.9} hexacarbonyltantalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of sodium{(THF)4.9} hexacarbonyltantalate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of sodium{(THF)4.9} hexacarbonyltantalate

There total 1 articles about sodium{(THF)4.9} hexacarbonyltantalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 67292-38-0
tetraethylammonium hexacarbonyltantalate

: 143-66-8
sodium tetraphenyl borate

: 15602-40-1
Na⁽¹⁺⁾*Ta(CO)6^(1-) = Na(Ta(CO)6)

: 12099-10-4
tetraethylammonium tetraphenylborate

Guidance literature:: In methanol; a methanolic slurry of the tantalate treating with a soln. of NaBPh4, stirring for 0.5 h at 40°C and for 1.5 h at 25°C, ammonium borate filtering off, filtrate evapg. to dryness, dissolving in Et2O, filtering, evapg., washing with pentane; identified by elem. anal. and IR spectrum;

Reference yield: 84.0%

: 15602-40-1
sodium hexacarbonyltantalate*THF

: 948-43-6
N-methylacridinium iodide

: {octacarbonyl(tantalum)2(μ-I)3}(1-)

: 3295-69-0
10,10'-dimethyl-9,10,9',10'-tetrahydro-[9,9']biacridinyl

Guidance literature:: In tetrahydrofuran; byproducts: CO; React. of starting materials in THF (N2 or Ar).;
DOI:10.1021/om00095a011

Reference yield: 79.0%

: 15602-40-1
sodium hexacarbonyltantalate*THF

: 18820-83-2
pyridine hydroiodide

: 112713-58-3
tetracarbonyl{1,2-bis(diphenylphosphino)ethane}iodotantalum

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

Guidance literature:: With C₂H₄(P(C₆H₅)2)2; In tetrahydrofuran; toluene; byproducts: C5H5N, CO, H2; Treating of suspn. of diphos and (H-py)I in THF with Ta-complex at room temp. under a CO atmosphere.; Immediate react. with evolution of CO and H2 (gas chromy.) obsd. Stirring (2 h, room temp.), removal of THF (vac., room temp.), dissolving of residue (toluene, CO), stirring (2 h), filtn., treating with n-heptane. Sepn. of microcryst., elem. anal.;
DOI:10.1021/om00095a011