N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide

Base Information

• Chemical Name: N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide
• CAS No.: 1411774-94-1
• Molecular Formula: C₂₄H₂₅NO₃S
• Molecular Weight: 407.533
• Mol file: 1411774-94-1.mol

Synonyms:N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide

Chemical Property of N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide

There total 4 articles about N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-diphenyl-4-pentenylamine (53001-06-2) + 4-methoxy-phenyl-sulphonyl chloride (98-68-0) → N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide (1411774-94-1)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 25 ℃; for 24h;

DOI:10.1002/anie.201208471

Reference yield:

Diphenylacetonitrile (86-29-3) → N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide (1411774-94-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 25 °C

1.2: 25 °C

2.1: lithium aluminium tetrahydride / diethyl ether / 0 - 25 °C

3.1: pyridine / dichloromethane / 24 h / 0 - 25 °C

With pyridine; lithium aluminium tetrahydride; sodium hydride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/anie.201208471

Reference yield:

2,2-diphenyl-pent-4-enenitrile (5558-71-4) → N-(2,2-diphenylpent-4-en-1-yl)-4-methoxybenzene-1-sulfonamide (1411774-94-1)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 0 - 25 °C

2: pyridine / dichloromethane / 24 h / 0 - 25 °C

With pyridine; lithium aluminium tetrahydride; In diethyl ether; dichloromethane;

DOI:10.1002/anie.201208471

upstream raw materials:

2,2-diphenyl-pent-4-enenitrile

Diphenylacetonitrile

chlorobenzene

2,2-diphenyl-4-pentenylamine