ethyl 2-amino-5-ethylbenzoate

Base Information

• Chemical Name: ethyl 2-amino-5-ethylbenzoate
• CAS No.: 2475-78-7
• Molecular Formula: C₁₁H₁₅NO₂
• Molecular Weight: 193.246

Synonyms:ethyl 2-amino-5-ethylbenzoate

Chemical Property of ethyl 2-amino-5-ethylbenzoate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

methyl2-amino-5-ethylbenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of ethyl 2-amino-5-ethylbenzoate

There total 5 articles about ethyl 2-amino-5-ethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

ethanol (64-17-5) + 2-amino-5-ethylbenzoic acid (2475-82-3) → ethyl 2-amino-5-ethylbenzoate (2475-78-7)

Guidance literature:

With hydrogenchloride; Reflux;

Reference yield:

5-ethyl-1H-indole-2,3-dione (96202-56-1) → ethyl 2-amino-5-ethylbenzoate (2475-78-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide; dihydrogen peroxide / water / 1 h / 15 - 20 °C

2: hydrogenchloride / Reflux

With hydrogenchloride; dihydrogen peroxide; sodium hydroxide; In water;

Reference yield:

acetophenone (98-86-2) → ethyl 2-amino-5-ethylbenzoate (2475-78-7)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium sulfate; hydroxylamine hydrochloride; hydrogenchloride / water / 0.17 h / Heating

2: sulfuric acid / 0.17 h / 50 - 75 °C

3: sodium hydroxide; dihydrogen peroxide / water / 1 h / 15 - 20 °C

4: hydrogenchloride / Reflux

With hydrogenchloride; sulfuric acid; hydroxylamine hydrochloride; dihydrogen peroxide; sodium sulfate; sodium hydroxide; In water;

upstream raw materials:

5-ethyl-1H-indole-2,3-dione

acetophenone

N-(4-ethylphenyl)-2-(hydroxyimino)acetamide

ethanol

Downstream raw materials:

5-ethyl-2-methanesulfonamidobenzoic acid

C₁₁H₁₅NO₄S

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