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Technology Process of [BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3

[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3

Base Information
  • Chemical Name:[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3
  • CAS No.:1334305-70-2
  • Molecular Formula:CF3O3S*C28H32BFN3
  • Molecular Weight:589.462
  • Hs Code.:
[BF(C<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)3NC<sub>6</sub>H<sub>4</sub>C(C<sub>4</sub>H(CH<sub>3</sub>)2N)2)]<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>=[BF(C<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)3NC<sub>6</sub>H<sub>4</sub>C(C<sub>4</sub>H(CH<sub>3</sub>)2N)2)]O<sub>3</sub>SCF<sub>3</sub>

Synonyms:[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3

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Chemical Property of [BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3
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Technology Process of [BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3

There total 7 articles about [BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide
1357002-73-3

10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

methyl trifluoromethanesulfonate
333-27-7

methyl trifluoromethanesulfonate

[BF(C<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)3NC<sub>6</sub>H<sub>4</sub>C(C<sub>4</sub>H(CH<sub>3</sub>)2N)2)]<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>=[BF(C<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)3NC<sub>6</sub>H<sub>4</sub>C(C<sub>4</sub>H(CH<sub>3</sub>)2N)2)]O<sub>3</sub>SCF<sub>3</sub>
1334305-70-2

[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3

Guidance literature:
In dichloromethane; Inert atmosphere;
DOI:10.1039/c1cc13089g

Reference yield:

2,4-dimethyl-1H-pyrrole
625-82-1

2,4-dimethyl-1H-pyrrole

[BF(C<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)3NC<sub>6</sub>H<sub>4</sub>C(C<sub>4</sub>H(CH<sub>3</sub>)2N)2)]<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>=[BF(C<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)3NC<sub>6</sub>H<sub>4</sub>C(C<sub>4</sub>H(CH<sub>3</sub>)2N)2)]O<sub>3</sub>SCF<sub>3</sub>
1334305-70-2

[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3

Guidance literature:
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere
1.2: 0.25 h / 20 °C / Inert atmosphere
1.3: 20 °C / Inert atmosphere
2.1: potassium hydrogen difluoride / tetrahydrofuran / 24 h / Inert atmosphere
3.1: dichloromethane / Inert atmosphere
With potassium hydrogen difluoride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1cc13089g

Reference yield:

phenylborondichloride
873-51-8

phenylborondichloride

[BF(C<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)3NC<sub>6</sub>H<sub>4</sub>C(C<sub>4</sub>H(CH<sub>3</sub>)2N)2)]<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>=[BF(C<sub>6</sub>H<sub>5</sub>)((CH<sub>3</sub>)3NC<sub>6</sub>H<sub>4</sub>C(C<sub>4</sub>H(CH<sub>3</sub>)2N)2)]O<sub>3</sub>SCF<sub>3</sub>
1334305-70-2

[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[BF(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3

Guidance literature:
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere
1.2: 0.25 h / 20 °C / Inert atmosphere
1.3: 20 °C / Inert atmosphere
2.1: potassium hydrogen difluoride / tetrahydrofuran / 24 h / Inert atmosphere
3.1: dichloromethane / Inert atmosphere
With potassium hydrogen difluoride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1cc13089g
upstream raw materials:

2,4-dimethyl-1H-pyrrole

[B(OH)(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[B(OH)(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3

10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

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