di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

Base Information

Chemical Name:di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate
CAS No.:934622-42-1
Molecular Formula:C₃₅H₄₅N₆O₉P
Molecular Weight:724.751
Hs Code.:

Synonyms:di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

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Chemical Property of di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

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Technology Process of di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

There total 9 articles about di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 913239-31-3
di-(4-acetamidophenyl) 1-(benzyloxycarbonylamino)-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

: 934622-42-1
di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 8h;
DOI:10.1021/jm060622g

Reference yield:

: 934622-38-5
benzyl 1-(bis(4-acetamidophenoxy)phosphoryl)-2-(4-amino-phenyl)ethylcarbamate

: 934622-42-1
di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / acetonitrile / Heating

2: H₂ / Pd/C / methanol / 8 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1021/jm060622g

Reference yield:

: 913239-30-2
di-(4-acetamidophenyl)-1-(benzyloxycarbonylamino)-2-(4-tert-butyloxycarbonylaminophenyl)ethanephosphonate

: 934622-42-1
di(4-acetamidophenyl) 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: TFA / CH₂Cl₂ / 3 h / 20 °C

2: Et₃N / acetonitrile / Heating

3: H₂ / Pd/C / methanol / 8 h / 20 °C

With hydrogen; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm060622g