trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester

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Chemical Name:trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester
CAS No.:790661-74-4
Molecular Formula:C₁₃H₁₄F₃NO₅S₂
Molecular Weight:385.385
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester

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Chemical Property of trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester

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Technology Process of trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester

There total 1 articles about trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 118429-46-2
1-(4-methylphenyl)sulfonyl-5-methyl-2-pyrrolidinone

: 790661-74-4
trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester

Guidance literature:: 1-(4-methylphenyl)sulfonyl-5-methyl-2-pyrrolidinone; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 1.5h;

N,N-phenylbistrifluoromethane-sulfonimide; In tetrahydrofuran; toluene; at -78 - 0 ℃;
DOI:10.1021/jo0489263

Reference yield: 77.0%

: 201230-82-2
carbon monoxide

: 104376-24-1,59239-44-0
(E)-1-pentenylboronic acid

: 790661-74-4
trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester

: (2E)-1-[5-methyl-1-(4-methylphenylsulfonyl)-4,5-dihydro-1H-pyrrol-2-yl]hex-2-en-1-one

: C₁₇H₂₃NO₂S

Guidance literature:: With triphenylphosphine; cesium fluoride; palladium diacetate; In tetrahydrofuran; at 18 - 22 ℃; for 18h; under 760.051 Torr;
DOI:10.1002/ejoc.200601089

Reference yield: 63.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 790661-74-4
trifluoromethanesulfonic acid 5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrol-2-yl ester

: 853356-43-1
(+/-)-5-methyl-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrrole-2-carboxylic acid methyl ester

Guidance literature:: With triethylamine; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 40 ℃; for 4h;
DOI:10.1021/jo0504058