phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester

Base Information

• Chemical Name: phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester
• CAS No.: 906072-79-5
• Molecular Formula: C₂₆H₂₁N₂O₈P
• Molecular Weight: 520.435
• Mol file: 906072-79-5.mol

Synonyms:phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester

Chemical Property of phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester

There total 1 articles about phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tris(p-nitrophenyl)phosphate (3871-20-3) + 2,2-diphenyl ethanol (1883-32-5) → phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester (906072-79-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; for 3h;

DOI:10.1021/ja0619253

Reference yield:

phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester (906072-79-5) → bis-N,N-(p-nitrophenyl-2,2-diphenylethyl-12-aminododecyl phosphate)-2,6-pyridine dicarbamide (906072-83-1)

Guidance literature:

Multi-step reaction with 3 steps

1: DBU / toluene

2: trifluoroacetic acid / CH₂Cl₂ / 0.33 h

3: triethylamine / CHCl₃ / 3 h

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid; In dichloromethane; chloroform; toluene;

DOI:10.1021/ja0619253

Reference yield:

phosphoric acid 2,2-diphenyl-ethyl ester bis-(4-nitro-phenyl) ester (906072-79-5) → bis-N,N-(p-nitrophenyl-2,2-diphenylethyl-12-aminododecyl phosphate)-2,5-dimethoxyterephthalamide (906072-82-0)

Guidance literature:

Multi-step reaction with 3 steps

1: DBU / toluene

2: trifluoroacetic acid / CH₂Cl₂ / 0.33 h

3: triethylamine / CHCl₃ / 3 h

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid; In dichloromethane; chloroform; toluene;

DOI:10.1021/ja0619253

upstream raw materials:

tris(p-nitrophenyl)phosphate

2,2-diphenyl ethanol

Downstream raw materials:

6-(tert-butylcarbamoyl)hexyl-2,2-diphenylethyl-4-nitrophenyl phosphate

12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate

bis-N,N-(p-nitrophenyl-2,2-diphenylethyl-6-aminododecyl phosphate)-2,6-pyridine dicarbamide

bis-N,N-(p-nitrophenyl-2,2-diphenylethyl-12-aminododecyl phosphate)fumaramide