12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate

Base Information

Chemical Name:12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate
CAS No.:906072-85-3
Molecular Formula:C₃₇H₅₁N₂O₈P
Molecular Weight:682.794
Hs Code.:

Synonyms:12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate

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Chemical Property of 12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate

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Technology Process of 12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate

There total 6 articles about 12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3871-20-3
tris(p-nitrophenyl)phosphate

: 906072-85-3
12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / DBU / CHCl₃ / 3 h

2: DBU / toluene

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; toluene;
DOI:10.1021/ja0619253

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 906072-85-3
12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / triethylamine / methanol / 60 °C

2: 84 percent / Red-Al / tetrahydrofuran; toluene / 1 h

3: DBU / toluene

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/ja0619253

Reference yield:

: 1883-32-5
2,2-diphenyl ethanol

: 906072-85-3
12-(tert-butylcarbamoyl)dodecyl-4-nitrophenyl-2,2-diphenylethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / DBU / CHCl₃ / 3 h

2: DBU / toluene

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; toluene;
DOI:10.1021/ja0619253