2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II)

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Chemical Name:2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II)
CAS No.:131214-92-1
Molecular Formula:C₄₄H₂₀AgBr₈N₄
Molecular Weight:1351.77
Hs Code.:

Synonyms:2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II)

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Chemical Property of 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II)

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Technology Process of 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II)

There total 3 articles about 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 14641-64-6
silver(II) meso-tetraphenylporphyrin

: 131214-92-1
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II)

Guidance literature:: With bromine; In chloroform; at 25 ℃; for 73h; Time;
DOI:10.1142/S1088424616500462

Reference yield: 85.0%

: 2,3,7,8,12,13,17,18-octobromo-5,10,15,20-tetraphenyl, 21H,23H-porphyrin

: 563-63-3
silver(I) acetate

: 131214-92-1
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II)

Guidance literature:: In chloroform; acetic acid; H2OBP in chloroform and Ag(CH3COO) in acetic acid were mixed,stirred for 30min; solvent was evapd. under reduced pressure, residue was dissolved in CHCl3, mixt. was washed with water; the org. layer was dried over Na2SO4 product was obtained on evapn. of the solvent; chromd. on basic alumina;

Reference yield:

: 917-23-7,20998-75-8
5,15,10,20-tetraphenylporphyrin

: 131214-92-1
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato silver(II)

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 3 h / Reflux

2: bromine / chloroform / 73 h / 25 °C

With bromine; In chloroform; acetic acid;
DOI:10.1142/S1088424616500462