methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate

Base Information

Chemical Name:methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate
CAS No.:1613483-84-3
Molecular Formula:C₂₆H₂₆O₈
Molecular Weight:466.488
Hs Code.:

Synonyms:methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate

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Chemical Property of methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate

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Technology Process of methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate

There total 3 articles about methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 1180491-77-3
methyl 3-(2-(3,5-dimethoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate

: 1613483-84-3
methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium hydride; In tetrahydrofuran; mineral oil; at 120 ℃; for 2h;
DOI:10.1021/jo500885w

Reference yield:

: 19520-74-2
3-hydroxy-5-methoxy-benzoic acid methyl ester

: 1613483-84-3
methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 2 h / 80 °C

2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 120 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium hydride; potassium carbonate; In tetrahydrofuran; acetone; mineral oil;
DOI:10.1021/jo500885w

Reference yield:

: 50841-50-4
(2-bromo-1-(3,5-dimethoxyphenyl)ethanone)

: 1613483-84-3
methyl 3-(2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-2-oxoethoxy)-5-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 2 h / 80 °C

2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 120 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium hydride; potassium carbonate; In tetrahydrofuran; acetone; mineral oil;
DOI:10.1021/jo500885w