V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2⁽¹⁺⁾*ClO₄^(1-)=[V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2](ClO₄)

Base Information

Chemical Name:V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2⁽¹⁺⁾*ClO₄^(1-)=[V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2](ClO₄)
CAS No.:202534-99-4
Molecular Formula:C₄₅H₅₉N₄O₁₆V₄*ClO₄
Molecular Weight:1215.2
Hs Code.:

V<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CC<sub>2</sub>H<sub>5</sub>)7(C<sub>12</sub>H<sub>12</sub>N<sub>2</sub>)2<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=[V<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CC<sub>2</sub>H<sub>5</sub>)7(C<sub>12</sub>H<sub>12</sub>N<sub>2</sub>)2](ClO<sub>4</sub>)

Synonyms:V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2⁽¹⁺⁾*ClO₄^(1-)=[V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2](ClO₄)

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Chemical Property of V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2⁽¹⁺⁾*ClO₄^(1-)=[V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2](ClO₄)

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Technology Process of V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2⁽¹⁺⁾*ClO₄^(1-)=[V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2](ClO₄)

There total 1 articles about V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2⁽¹⁺⁾*ClO₄^(1-)=[V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1134-35-6
4,4'-dimethyl-2,2'-bipyridines

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Vanadium (III) chloride-(tris-tetrahydrofuran)

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sodium proprionate

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tetrabutylammonium perchlorate

: 202534-99-4
V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2⁽¹⁺⁾*ClO₄^(1-)=[V₄O₂(O₂CC₂H₅)7(C₁₂H₁₂N₂)2](ClO₄)

: 7647-14-5
sodium chloride

Guidance literature:: In acetone; inert atmosphere, Schlenk techniques; slurry (V- and Na-compds., bpy and solvent) stirring overnight at room temp., NaCl ppt. filtration off, NBu4ClO4 addn. to filtrate, solvent removal (vac.), residue washing (Et2O), redissoln. (acetone); distn. (A4 molecular sieve), pptn. on large excess Et2O addn., ppt. filtration off, washing (Et2O), vac. drying; elem. anal.;
DOI:10.1021/ja9732439