tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate
CAS No.:1124215-20-8
Molecular Formula:C₁₈H₂₆FN₃O₃
Molecular Weight:351.421
Hs Code.:

Synonyms:tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate

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Chemical Property of tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate

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Technology Process of tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate

There total 1 articles about tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 455-87-8
4-amino-3-fluorobenzoic acid

: 674792-07-5
2,2-dimethyl-piperazine-1-carboxylic acid tert-butyl ester

: 1124215-20-8
tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate

Guidance literature:: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; In dichloromethane; ethyl acetate; for 2h;

Reference yield:

: 1124215-20-8
tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate

: 1124215-15-1
(4-amino-3-fluorophenyl)(3,3-dimethylpiperazin-1-yl)methanone

Guidance literature:: tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate; With trifluoroacetic acid; In dichloromethane; for 1h;

With ammonia; In methanol;

Reference yield:

: 1124215-20-8
tert-butyl 4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazine-1-carboxylate

: 1124215-23-1
3-((4-(4-amino-3-fluorobenzoyl)-2,2-dimethylpiperazin-1-yl)methyl)-N-tert-butyl-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h

2: triethylamine / sodium iodide / dichloromethane; acetonitrile / 3 h / Reflux

With triethylamine; trifluoroacetic acid; sodium iodide; In dichloromethane; acetonitrile;