5,5-(ethylenedioxy)-5-phenylpentanal

Base Information

Chemical Name:5,5-(ethylenedioxy)-5-phenylpentanal
CAS No.:165613-10-5
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:

Synonyms:5,5-(ethylenedioxy)-5-phenylpentanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5-(ethylenedioxy)-5-phenylpentanal

Chemical Property:

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Technology Process of 5,5-(ethylenedioxy)-5-phenylpentanal

There total 8 articles about 5,5-(ethylenedioxy)-5-phenylpentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 17851-44-4
ethyl 6-phenyl 5,5-(ethylenedioxy)hexanoate

: 165613-10-5
5,5-(ethylenedioxy)-5-phenylpentanal

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃;
DOI:10.1021/ol015520t

Reference yield:

: 17851-47-7
4-(2-phenyl-1,3-dioxolan-2-yl)-1-butanol

: 165613-10-5
5,5-(ethylenedioxy)-5-phenylpentanal

Guidance literature:: With phosphorus pentoxide; dimethyl sulfoxide; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, room temperature, 2 h, 2.) CH₂Cl₂, room temperature, 4h;

Reference yield:

: 73172-56-2
ethyl 4-benzoylbutanoate

: 165613-10-5
5,5-(ethylenedioxy)-5-phenylpentanal

Guidance literature:: Multi-step reaction with 3 steps

1: pTsOH / benzene / Heating

2: LiAlH₄ / tetrahydrofuran / 0 °C

3: PDC / CH₂Cl₂ / 20 °C

With lithium aluminium tetrahydride; dipyridinium dichromate; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ol0159928