4-Oxo-3-phenylselanyl-cyclohexane-1,1,3-tricarboxylic acid di-tert-butyl ester 4-methoxy-benzyl ester

Base Information

Chemical Name:4-Oxo-3-phenylselanyl-cyclohexane-1,1,3-tricarboxylic acid di-tert-butyl ester 4-methoxy-benzyl ester
CAS No.:180588-00-5
Molecular Formula:C₃₁H₃₈O₈Se
Molecular Weight:617.598
Hs Code.:

Synonyms:4-Oxo-3-phenylselanyl-cyclohexane-1,1,3-tricarboxylic acid di-tert-butyl ester 4-methoxy-benzyl ester

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Chemical Property of 4-Oxo-3-phenylselanyl-cyclohexane-1,1,3-tricarboxylic acid di-tert-butyl ester 4-methoxy-benzyl ester

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Technology Process of 4-Oxo-3-phenylselanyl-cyclohexane-1,1,3-tricarboxylic acid di-tert-butyl ester 4-methoxy-benzyl ester

There total 3 articles about 4-Oxo-3-phenylselanyl-cyclohexane-1,1,3-tricarboxylic acid di-tert-butyl ester 4-methoxy-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133208-88-5
4-methoxybenzyl acrylate

: 180588-00-5
4-Oxo-3-phenylselanyl-cyclohexane-1,1,3-tricarboxylic acid di-tert-butyl ester 4-methoxy-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) THF, 2.) THF, 40 min

2: 1.) pyridine / 1.) CH₂Cl₂, 15 min, 2.) CH₂Cl₂, 0 deg C, 1 h

With pyridine; sodium hydride;
DOI:10.1021/jo960245n

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 180588-00-5
4-Oxo-3-phenylselanyl-cyclohexane-1,1,3-tricarboxylic acid di-tert-butyl ester 4-methoxy-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride / 1.) THF, 40-48 deg C, 15 min, 2.) THF, -78 deg C, 2 h

2: 1.) sodium hydride / 1.) THF, 2.) THF, 40 min

3: 1.) pyridine / 1.) CH₂Cl₂, 15 min, 2.) CH₂Cl₂, 0 deg C, 1 h

With pyridine; sodium hydride;
DOI:10.1021/jo960245n