methylene bismethyl>cyclohexanecarboxylate>

Base Information

Chemical Name:methylene bismethyl>cyclohexanecarboxylate>
CAS No.:87611-41-4
Molecular Formula:C₂₇H₄₆N₂O₈
Molecular Weight:526.671
Hs Code.:

methylene bis<trans-4-<<(tert-butoxycarbonyl)amino>methyl>cyclohexanecarboxylate>

Synonyms:methylene bismethyl>cyclohexanecarboxylate>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methylene bismethyl>cyclohexanecarboxylate>

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Technology Process of methylene bismethyl>cyclohexanecarboxylate>

There total 3 articles about methylene bismethyl>cyclohexanecarboxylate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 87611-41-4
methylene bismethyl>cyclohexanecarboxylate>

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaOH / H₂O; 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: 1.) tetrabutylammonium hydrogen sulfate (QHSO₄), 2 M aq. NaOH / 2.) reflux, 6 d

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In water; tert-butyl alcohol;
DOI:10.1021/jm00154a004

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 87611-41-4
methylene bismethyl>cyclohexanecarboxylate>

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaOH / H₂O; 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: 1.) tetrabutylammonium hydrogen sulfate (QHSO₄), 2 M aq. NaOH / 2.) reflux, 6 d

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In water; tert-butyl alcohol;
DOI:10.1021/jm00154a004

Reference yield:

: 75-09-2
dichloromethane

: 27687-14-5
trans 4-(tert-butyloxycarbonylamino)methylcyclohexanecarboxylic acid

: 87611-41-4
methylene bismethyl>cyclohexanecarboxylate>

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; Yield given. Multistep reaction; 2.) reflux, 6 d;
DOI:10.1021/jm00154a004