Technology Process of 2,4-dibenzyloxyphenylacetic acid p-nitrophenyl ester
There total 6 articles about 2,4-dibenzyloxyphenylacetic acid p-nitrophenyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 92 percent / K2CO3 / acetone / 24 h / Heating
2: 91 percent / Tl(NO3)3*3H2O, 70percent HClO4 / 1.33 h / Ambient temperature
3: 98 percent / LiOH*H2O / methanol; H2O / Ambient temperature
4: 86 percent / dicyclohexylcarbodiimide (DCC) / acetone; ethyl acetate / 1) 0 deg C, 12 h, 2) slowly to r.t.
With
lithium hydroxide; perchloric acid; potassium carbonate; dicyclohexyl-carbodiimide; thallium(III) nitrate;
In
methanol; water; ethyl acetate; acetone;
DOI:10.1016/S0040-4020(01)87944-8
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / Tl(NO3)3*3H2O, 70percent HClO4 / 1.33 h / Ambient temperature
2: 98 percent / LiOH*H2O / methanol; H2O / Ambient temperature
3: 86 percent / dicyclohexylcarbodiimide (DCC) / acetone; ethyl acetate / 1) 0 deg C, 12 h, 2) slowly to r.t.
With
lithium hydroxide; perchloric acid; dicyclohexyl-carbodiimide; thallium(III) nitrate;
In
methanol; water; ethyl acetate; acetone;
DOI:10.1016/S0040-4020(01)87944-8
