N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide

Base Information

Chemical Name:N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide
CAS No.:1254315-01-9
Molecular Formula:C₂₅H₁₂BrClF₁₂N₂O₃
Molecular Weight:731.72
Hs Code.:

Synonyms:N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide

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Chemical Property of N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide

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Technology Process of N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide

There total 7 articles about N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79538-29-7
2,4,6-trifluorobenzoyl chloride

: 1254318-25-6
3-amino-N-[2-ethyl-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-6-methylphenyl]-2-methoxy benzamide

: 1254315-01-9
N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 573-54-6
2-bromo-3-nitro-benzoic acid

: 1254315-01-9
N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 1 h / 100 °C

2.1: pyridine / tetrahydrofuran / 18 h / 20 °C / Reflux

2.2: 41 h / 20 °C

3.1: potassium carbonate / 16 h / 20 °C

4.1: hydrogenchloride; tin(ll) chloride / water; isopropyl alcohol / 0 - 80 °C

4.2: pH 7 - 8

5.1: pyridine / tetrahydrofuran / 2 h / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; potassium carbonate; tin(ll) chloride; N,N-dimethyl-formamide; In tetrahydrofuran; water; isopropyl alcohol; toluene;

Reference yield:

: 317-46-4
2-fluoro-3-nitro-benzoic acid

: 1254315-01-9
N-{3-[2-bromo-6-chloro-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-phenylcarbamoyl]-2-methoxyphenyl}-2,4,6-trifluorobenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C / Reflux

2.1: pyridine / tetrahydrofuran / 6 h / 20 °C / Reflux

3.1: potassium carbonate / 16 h / 20 °C

4.1: hydrogenchloride; tin(ll) chloride / water; isopropyl alcohol / 0 - 80 °C

4.2: pH 7 - 8

5.1: pyridine / tetrahydrofuran / 2 h / 20 °C

With pyridine; hydrogenchloride; oxalyl dichloride; potassium carbonate; tin(ll) chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;