2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester

Base Information

Chemical Name:2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester
CAS No.:602280-43-3
Molecular Formula:C₂₀H₁₆Cl₂N₂O₃
Molecular Weight:403.265
Hs Code.:

Synonyms:2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester

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Chemical Property of 2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester

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Technology Process of 2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester

There total 4 articles about 2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 79-37-8
oxalyl dichloride

: benzyl 2-(1-cyano-2-phenylethylamino)acetate

: 602280-43-3
2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester

Guidance literature:: benzyl 2-(1-cyano-2-phenylethylamino)acetate; With hydrogenchloride; In diethyl ether; for 0.0833333h; Inert atmosphere;

oxalyl dichloride; In 1,2-dimethoxyethane; at 170 ℃; for 0.166667h; Microwave irradiation; Autoclave;
DOI:10.1039/b905501k

Reference yield: 38.0%

: 79-37-8
oxalyl dichloride

: 7677-24-9
trimethylsilyl cyanide

: 1738-68-7
Gly-OBz

: 122-78-1
phenylacetaldehyde

: 602280-43-3
2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester

Guidance literature:: trimethylsilyl cyanide; Gly-OBz; phenylacetaldehyde; In dichloromethane;

oxalyl dichloride; In 1,2-dichloro-benzene;
DOI:10.1016/S0960-894X(03)00410-4

Reference yield:

: 7677-24-9
trimethylsilyl cyanide

: 122-78-1
phenylacetaldehyde

: 2462-31-9
benzyl 2-aminoacetate hydrochloride

: 602280-43-3
2-(6-benzyl-3,5-dichloro-2-oxopyrazin-1(2H)-yl)acetic acid benzyl ester

Guidance literature:: trimethylsilyl cyanide; phenylacetaldehyde; benzyl 2-aminoacetate hydrochloride; In 1,2-dimethoxyethane; Sealed vial; Microwave irradiation;

With hydrogenchloride; In diethyl ether; Sealed vial; Microwave irradiation;

With oxalyl dichloride; In 1,2-dimethoxyethane; Sealed vial; Microwave irradiation; Heating;
DOI:10.1016/j.bmc.2010.06.101