isoperillyl chloroformate

Base Information

Chemical Name:isoperillyl chloroformate
CAS No.:1383381-39-2
Molecular Formula:C₁₁H₁₅ClO₂
Molecular Weight:214.692
Hs Code.:

Synonyms:isoperillyl chloroformate

Suppliers and Price of isoperillyl chloroformate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isoperillyl chloroformate

Chemical Property:

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Technology Process of isoperillyl chloroformate

There total 8 articles about isoperillyl chloroformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-44-5
phosgene

: 110299-94-0
4-isopropylidene cyclohex-1-enyl methanol

: 1383381-39-2
isoperillyl chloroformate

Guidance literature:: With potassium carbonate; In toluene; at 10 - 20 ℃; for 10.75h; Inert atmosphere;

Reference yield:

: 19620-36-1
4-(propan-2-ylidene)cyclohexan-1-one

: 1383381-39-2
isoperillyl chloroformate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere

2.1: aluminum isopropoxide / toluene / 7 h / Reflux

2.2: 20 °C

3.1: potassium carbonate / toluene / 10.75 h / 10 - 20 °C / Inert atmosphere

With potassium tert-butylate; aluminum isopropoxide; potassium carbonate; In dimethyl sulfoxide; toluene;

Reference yield:

: 1383381-36-9
trifluoromethanesulfonic acid 4-isopropylidenecyclohex-1-enyl ester

: 1383381-39-2
isoperillyl chloroformate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / 1,3-bis-(diphenylphosphino)propane; palladium diacetate / N,N-dimethyl-formamide / 5 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

2.2: 5 °C

3.1: potassium carbonate / toluene / 10.75 h / 10 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;