4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide)

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Chemical Name:4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide)
CAS No.:1383381-41-6
Molecular Formula:C₄₀H₄₄F₃N₃O₆S
Molecular Weight:751.867
Hs Code.:

Synonyms:4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide)

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Chemical Property of 4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide)

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Technology Process of 4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide)

There total 8 articles about 4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 457639-26-8
Dimethyl-celecoxib

: 1383381-39-2
isoperillyl chloroformate

: 1383381-41-6
4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide)

Guidance literature:: With potassium carbonate; In acetone; for 4h; Inert atmosphere; Reflux;

Reference yield:

: 19620-36-1
4-(propan-2-ylidene)cyclohexan-1-one

: 1383381-41-6
4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide)

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere

2.1: aluminum isopropoxide / toluene / 7 h / Reflux

2.2: 20 °C

3.1: potassium carbonate / toluene / 10.75 h / 10 - 20 °C / Inert atmosphere

4.1: potassium carbonate / acetone / 4 h / Inert atmosphere; Reflux

With potassium tert-butylate; aluminum isopropoxide; potassium carbonate; In dimethyl sulfoxide; acetone; toluene;

Reference yield:

: 1383381-36-9
trifluoromethanesulfonic acid 4-isopropylidenecyclohex-1-enyl ester

: 1383381-41-6
4-(bis-N,N’-4-isopropylidene cyclohex-1-enylmethyloxycarbonyl[5-(2,5-dimethylphenyl)-3-trifluoromethylpyrazol-1-yl]benzenesulfonamide)

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / 1,3-bis-(diphenylphosphino)propane; palladium diacetate / N,N-dimethyl-formamide / 5 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

2.2: 5 °C

3.1: potassium carbonate / toluene / 10.75 h / 10 - 20 °C / Inert atmosphere

4.1: potassium carbonate / acetone / 4 h / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;