5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-diene-3-yl-methoxymethaneimine

Base Information

• Chemical Name: 5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-diene-3-yl-methoxymethaneimine
• CAS No.: 1024005-29-5
• Molecular Formula: C₁₆H₁₅F₂N₃O
• Molecular Weight: 303.311

Synonyms:5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-diene-3-yl-methoxymethaneimine

Chemical Property of 5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-diene-3-yl-methoxymethaneimine

Chemical Property:

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Technology Process of 5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-diene-3-yl-methoxymethaneimine

There total 1 articles about 5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-diene-3-yl-methoxymethaneimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

methanol (67-56-1) + 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbonitrile (1024005-25-1) → 5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-diene-3-yl-methoxymethaneimine (1024005-29-5)

Guidance literature:

methanol; 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbonitrile; With hydrogenchloride; In diethyl ether; at 0 - 5 ℃; for 25h;

With potassium hydroxide; water; In dichloromethane;

Reference yield: 82.0%

5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-diene-3-yl-methoxymethaneimine (1024005-29-5) + pivaloyl chloride (3282-30-2) → N1-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide (1024005-32-0)

Guidance literature:

With triethylamine; In toluene; at 0 - 35 ℃; for 48h;

Reference yield: 69.0%

5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-diene-3-yl-methoxymethaneimine (1024005-29-5) → 5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3-yl(imino)methylamine (1024005-36-4)

Guidance literature:

With ammonium chloride; In ethanol; for 4h; Heating / reflux;

upstream raw materials:

methanol

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbonitrile

Downstream raw materials:

N₁-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide

5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-yl(imino)methylamine

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