6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

Base Information

Chemical Name:6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide
CAS No.:1456906-53-8
Molecular Formula:C₃₃H₃₈ClN₃O₅
Molecular Weight:592.135
Hs Code.:

Synonyms:6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

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Technology Process of 6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

There total 1 articles about 6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 71989-26-9
Fmoc-Lys(tert-butoxycarbonyl)

: 104-86-9
4-chlorobenzylamine

: 1456906-53-8
6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/anie.201303999

Reference yield: 66.0%

: 1456906-53-8
6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

: 1456906-56-1
2-amino-6-(N-tert-butoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

Guidance literature:: With piperidine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/anie.201303999

Reference yield:

: 1456906-53-8
6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

: 1456906-61-8
6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / dichloromethane / 2 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

With piperidine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303999