6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

Base Information

Chemical Name:6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide
CAS No.:1456906-61-8
Molecular Formula:C₃₁H₃₆ClN₃O₄
Molecular Weight:550.098
Hs Code.:

Synonyms:6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

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Chemical Property of 6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

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Technology Process of 6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

There total 4 articles about 6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1456906-56-1
2-amino-6-(N-tert-butoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

: 92-92-2
biphenyl-4-carboxylic acid

: 1456906-61-8
6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/anie.201303999

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 1456906-61-8
6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

2: piperidine / dichloromethane / 2 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

With piperidine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303999

Reference yield:

: 1456906-53-8
6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

: 1456906-61-8
6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / dichloromethane / 2 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

With piperidine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303999