6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride

Base Information

Chemical Name:6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride
CAS No.:1456906-65-2
Molecular Formula:C₂₆H₂₈ClN₃O₂*ClH
Molecular Weight:486.441
Hs Code.:

Synonyms:6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride

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Chemical Property of 6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride

Chemical Property:

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Technology Process of 6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride

There total 5 articles about 6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1456906-61-8
6-(N-tert-butoxycarbonyl)amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

: 1456906-65-2
6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 0 - 20 ℃; for 2.5h;
DOI:10.1002/anie.201303999

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 1456906-65-2
6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

2: piperidine / dichloromethane / 2 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

4: hydrogenchloride / 1,4-dioxane; dichloromethane / 2.5 h / 0 - 20 °C

With piperidine; hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303999

Reference yield:

: 1456906-53-8
6-(N-tert-butoxycarbonyl)amino-2-(n-fluorenylmethoxycarbonyl)amino-N-(4-chlorobenzyl)hexaneamide

: 1456906-65-2
6-amino-2-(n-4-phenylbenzenecarbonyl)amino-N-(4-chlorobenzyl)hexaneamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / dichloromethane / 2 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

3: hydrogenchloride / 1,4-dioxane; dichloromethane / 2.5 h / 0 - 20 °C

With piperidine; hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303999