3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane

Base Information

Chemical Name:3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane
CAS No.:130220-15-4
Molecular Formula:C₃₁H₄₂O₄S₃Si
Molecular Weight:602.956
Hs Code.:

Synonyms:3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane

Suppliers and Price of 3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane

There total 6 articles about 3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 28519-50-8
potassium thiotosylate

: 130220-12-1
9-iodo-3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)nonane

: 130220-15-4
3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane

Guidance literature:: In water; acetone; for 20h; Ambient temperature;

Reference yield:

: 17494-61-0
((3-phenylpropyl)sulfonyl)benzene

: 130220-15-4
3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to 25 deg C

2: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, -78 deg C, 15 min, 2.) from -78 deg C to RT, 4 h

3: 88 percent / acetone; H₂O / 20 h / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In water; acetone;

Reference yield:

: 30134-12-4
phenyl 3-phenylpropyl sulfide

: 130220-15-4
3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-p-(toluenethiosulfonyl)nonane

Guidance literature:: Multi-step reaction with 4 steps

1: 80percent m-chloroperbenzoic acid / CH₂Cl₂ / 25 °C

2: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to 25 deg C

3: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, -78 deg C, 15 min, 2.) from -78 deg C to RT, 4 h

4: 88 percent / acetone; H₂O / 20 h / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; acetone;