(2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid

Base Information

Chemical Name:(2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid
CAS No.:1393646-06-4
Molecular Formula:C₂₆H₂₉NO₆
Molecular Weight:451.519
Hs Code.:

Synonyms:(2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid

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Chemical Property of (2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid

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Technology Process of (2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid

There total 4 articles about (2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353579-45-9
(2R,3S)-3-(benzyloxy)-3-(3-((benzyloxy)methyl)-2-methoxypyridin-4-yl)pentane-1,2-diol

: 1393646-06-4
(2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid

Guidance literature:: With sodium hypochlorite; sodium chlorite; potassium dihydrogenphosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; In acetonitrile; at 20 ℃;

Reference yield:

: 100-39-0
benzyl bromide

: 1393646-06-4
(2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / 1 h / Reflux; Inert atmosphere

2: hydrogenchloride / methanol / 20 °C

3: sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; potassium dihydrogenphosphate; water / acetonitrile / 20 °C

With hydrogenchloride; sodium hypochlorite; sodium chlorite; potassium dihydrogenphosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; sodium hydride; In methanol; acetonitrile;

Reference yield:

: 1353579-43-7
4-((S)-1-(benzyloxy)-1-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-propyl)-3-((benzyloxy)methyl)-2-methoxypyridine

: 1393646-06-4
(2S,3S)-3-benzyloxy-3-(3-benzyloxymethyl-2-methoxypyridin-4-yl)-2-hydroxypentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol / 20 °C

2: sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; potassium dihydrogenphosphate; water / acetonitrile / 20 °C

With hydrogenchloride; sodium hypochlorite; sodium chlorite; potassium dihydrogenphosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; In methanol; acetonitrile;