1,1-Dimethoxycyclobutane

Base Information

• Chemical Name: 1,1-Dimethoxycyclobutane
• CAS No.: 4415-90-1
• Molecular Formula: C₆H₁₂O₂
• Molecular Weight: 116.16
• European Community (EC) Number: 859-815-2
• Nikkaji Number: J1.026.525H
• Mol file: 4415-90-1.mol

Synonyms:1,1-dimethoxycyclobutane;4415-90-1;SCHEMBL1140153;AKOS026729624;AB89717;EN300-128645;Z1614786334

Chemical Property of 1,1-Dimethoxycyclobutane

Chemical Property:

• Vapor Pressure: 30.836mmHg at 25°C
• XLogP3: 0.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 116.083729621
• Heavy Atom Count: 8
• Complexity: 70.6

Purity/Quality:

97% ^*data from raw suppliers

1,1-dimethoxycyclobutane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1(CCC1)OC

Technology Process of 1,1-Dimethoxycyclobutane

There total 3 articles about 1,1-Dimethoxycyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methanol (67-56-1) + cyclobutanone (1191-95-3) → cyclobutanone dimethylacetal (4415-90-1)

Guidance literature:

With titanium tetrachloride; triethylamine; In dichloromethane; at 20 ℃; for 0.75h;

DOI:10.1016/S0040-4020(00)01001-2

Reference yield: 95.0%

cyclobutanone (1191-95-3) + trimethyl orthoformate (149-73-5) → cyclobutanone dimethylacetal (4415-90-1)

Guidance literature:

With montmorillonite K-10; In hexane; at 20 ℃;

DOI:10.1021/jo035295o

Reference yield:

→ cyclobutanone dimethylacetal (4415-90-1)

Guidance literature:

Cyclobutanon, Si(OMe)4,MeOH;

DOI:10.1021/jo00835a041

upstream raw materials:

methanol

cyclobutanone

trimethyl orthoformate

Downstream raw materials:

methanol

cyclobutanone